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Effect of Substrate Temperature and Gas Flow Ratio on The Nanocomposite TiAlBN Coating
Conference proceeding   Peer reviewed

Effect of Substrate Temperature and Gas Flow Ratio on The Nanocomposite TiAlBN Coating

Z. M. Rosli, W. L. Kwan and J. M. Juoi
AIP conference proceedings, Vol.1756(1), 020003
AIP Conference Proceedings
19/07/2016

Abstract

Metallurgy & Metallurgical Engineering Physical Sciences Physics Physics, Applied Science & Technology Technology
Nanocomposite TiAlBN (nc-TiAlBN) coatings were successfully deposited via RF magnetron sputtering by varying the nitrogen-to-total gas flow ratio (R-N), and substrate temperature (T-S). All coatings were deposited on AISI 316 substrates using single Ti-Al-BN hot-pressed disc as a target. The grain size, phases, and chemical composition of the coatings were evaluated using glancing angle X-ray diffraction analysis (GAXRD) and X-ray photoelectron spectroscopy (XPS). Results showed that the grains size of the deposited nc-TiAlBN coatings were in the range of 3.5 to 5.7 nm and reached a nitride saturation state as early as 15 % R-N. As the nitrogen concentration decreases, boron concentration increased from 9 at.% to 16.17 at.%. and thus, increase the TiB2 phase within the coatings. The T-S, however, showed no significant effect either on the crystallographic structure, grain size, or in the chemical composition of the deposited nc-TiAlBN coating.

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